Supercritical Carbon Dioxide Extraction of Microula sikkimensis Seed Oil

NWIPB OpenIR

	Supercritical Carbon Dioxide Extraction of Microula sikkimensis Seed Oil
	Lina, Shi 1,2; Fei, Ren 1,2; Xudong, Zhao 3; Yangong, Du 2; Fa, Han 1
	2010-10-01
发表期刊	JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY
ISSN	0003-021X
卷号	87 期号:10 页码:1221-1226
文章类型	Article
摘要	The seed oil of Microula sikkimensis had been intensively studied due to its pharmacological actions. In the present study, seed oil of Microula sikkimensis was extracted using supercritical fluid extraction (SFE). Determinations of the extracts composition were performed by gas chromatography (GC). An orthogonal array design (OAD), OA(9) (3(4)), was employed for optimization of the supercritical fluid extraction of the compound with regard to the various parameters. Four factors, namely pressure (21.0-27.0 MPa), the dynamic extraction time, temperature, and CO(2) flow rate of the supercritical fluid, were studied and optimized by a three-level OAD. The effects of the parameters on the yield of seed oil were studied using analysis of variance (ANOVA). The results revealed that the pressure had a significant effect on the yield of seed oil (p < 0.05), while the other three factors, i.e., CO(2) flow rate, dynamic extraction time and temperature, were not identified as significant factors under the selected conditions based on ANOVA. The results show that the best values for the extraction condition of seed oil was pressure 24.0 MPa, extraction time 3 h, temperature 45 A degrees C and a CO(2) flow rate 20 L/h in the 20-L vessel.; The seed oil of Microula sikkimensis had been intensively studied due to its pharmacological actions. In the present study, seed oil of Microula sikkimensis was extracted using supercritical fluid extraction (SFE). Determinations of the extracts composition were performed by gas chromatography (GC). An orthogonal array design (OAD), OA(9) (3(4)), was employed for optimization of the supercritical fluid extraction of the compound with regard to the various parameters. Four factors, namely pressure (21.0-27.0 MPa), the dynamic extraction time, temperature, and CO(2) flow rate of the supercritical fluid, were studied and optimized by a three-level OAD. The effects of the parameters on the yield of seed oil were studied using analysis of variance (ANOVA). The results revealed that the pressure had a significant effect on the yield of seed oil (p < 0.05), while the other three factors, i.e., CO(2) flow rate, dynamic extraction time and temperature, were not identified as significant factors under the selected conditions based on ANOVA. The results show that the best values for the extraction condition of seed oil was pressure 24.0 MPa, extraction time 3 h, temperature 45 A degrees C and a CO(2) flow rate 20 L/h in the 20-L vessel.
关键词	Microula Sikkimensis Supercritical Fluid Extraction Orthogonal Array Design
WOS标题词	Science & Technology ; Physical Sciences ; Life Sciences & Biomedicine
关键词[WOS]	FLUID EXTRACTION ; CO2
收录类别	SCI
语种	英语
WOS研究方向	Chemistry ; Food Science & Technology
WOS类目	Chemistry, Applied ; Food Science & Technology
WOS记录号	WOS:000281726200014
引用统计	被引频次：5[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	http://210.75.249.4/handle/363003/1646
专题	中国科学院西北高原生物研究所
作者单位	1.Chinese Acad Sci, NW Inst Plateau Biol, Xining 810001, Qinghai, Peoples R China 2.Chinese Acad Sci, Grad Univ, Beijing 100039, Peoples R China 3.QingHai Environm Monitoring Ctr, Xining 810007, Qinghai, Peoples R China
推荐引用方式 GB/T 7714	Lina, Shi,Fei, Ren,Xudong, Zhao,et al. Supercritical Carbon Dioxide Extraction of Microula sikkimensis Seed Oil[J]. JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY,2010,87(10):1221-1226.
APA	Lina, Shi,Fei, Ren,Xudong, Zhao,Yangong, Du,&Fa, Han.(2010).Supercritical Carbon Dioxide Extraction of Microula sikkimensis Seed Oil.JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY,87(10),1221-1226.
MLA	Lina, Shi,et al."Supercritical Carbon Dioxide Extraction of Microula sikkimensis Seed Oil".JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY 87.10(2010):1221-1226.

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