Knowledge Management System of Northwest Institute of Plateau Biology, CAS
| Compositional and Antioxidant Activity Analysis of Zanthoxylum bungeanum Seed Oil Obtained by Supercritical CO2 Fluid Extraction | |
| Xia, Lian1,2,3; You, Jinmao1,2; Li, Guoliang2,3; Sun, Zhiwei2,3; Suo, Yourui2 | |
| 2011 | |
| 发表期刊 | JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY
 |
| ISSN | 0003-021X |
| 卷号 | 88期号:1页码:23-32 |
| 文章类型 | Article |
| 摘要 | Supercritical CO2 fluid extraction (SFE-CO2)of Zanthoxylum bungeanum (Z. bungeanum) seed oil was investigated. To optimize the SFE process, three-level Box-Behnken factorial design and response surface methodology (RSM) were applied to optimize the extraction conditions, including pressure, temperature and amount of modifier. The optimum conditions were as follows: extraction pressure, 29.28 MPa; extraction temperature, 41.19; and the added amount of modifier, 10.94%. The experimental results showed that the maximum extraction yield was 21.85 ± 0.23% (n = 3) under the proposed conditions. The compositional analysis of Z. bungeanum seed oil was performed by HPLC-FLD-MS using a new labeling reagent of 2-(11H-benzo[a]carbazol-11-yl)-ethyl- 4-methyl benzenesulfonate (BCETS). The results indicated that the Z. bungeanum seed oil contained mainly unsaturated fatty acids, including C18:3, C22:6, C20:4, C18:2, C18:1 and C20:1, which accounted for 84.0% (mass percentage) of the total amount. The antioxidant activity of seed oil obtained by Box-Behnken design concerning the DPPH radical was investigated, and this indicated that the pressure and the amount of added modifier had positive effects on the antioxidant activity,; Supercritical CO2 fluid extraction (SFE-CO2) of Zanthoxylum bungeanum (Z. bungeanum) seed oil was investigated. To optimize the SFE process, three-level Box-Behnken factorial design and response surface methodology (RSM) were applied to optimize the extraction conditions, including pressure, temperature and amount of modifier. The optimum conditions were as follows: extraction pressure, 29.28 MPa; extraction temperature, 41.19 degrees C; and the added amount of modifier, 10.94%. The experimental results showed that the maximum extraction yield was 21.85 +/- 0.23% (n = 3) under the proposed conditions. The compositional analysis of Z. bungeanum seed oil was performed by HPLC-FLD-MS using a new labeling reagent of 2-(11H-benzo[a]carbazol-11-yl)-ethyl-4-methyl benzenesulfonate (BCETS). The results indicated that the Z. bungeanum seed oil contained mainly unsaturated fatty acids, including C18:3, C22:6, C20:4, C18: 2, C18: 1 and C20: 1, which accounted for 84.0% (mass percentage) of the total amount. The antioxidant activity of seed oil obtained by Box-Behnken design concerning the DPPH radical was investigated, and this indicated that the pressure and the amount of added modifier had positive effects on the antioxidant activity, but the effect of the temperature elevation is complicated, depending on the nature of the extracted contents. |
| 关键词 | Supercritical Co2 Fluid Extraction Zanthoxylum Bungeanum Seed Oil Fatty Acids Composition Hplc-fld-ms Antioxidant Activity |
| WOS标题词 | Science & Technology ; Physical Sciences ; Life Sciences & Biomedicine |
| 关键词[WOS] | CARBON-DIOXIDE EXTRACTION ; OPTIMIZATION ; CONSTITUENTS |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS研究方向 | Chemistry ; Food Science & Technology |
| WOS类目 | Chemistry, Applied ; Food Science & Technology |
| WOS记录号 | WOS:000287372200003 |
| 引用统计 | |
| 文献类型 | 期刊论文 |
| 条目标识符 | http://210.75.249.4/handle/363003/1992 |
| 专题 | 中国科学院西北高原生物研究所 |
| 作者单位 | 1.Qufu Normal Univ, Key Lab Life Organ Anal Shan Dong Prov, Coll Chem Sci, Qufu 273165, Peoples R China 2.Chinese Acad Sci, NW Plateau Inst Biol, Xining 810001, Peoples R China 3.Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China |
| 推荐引用方式 GB/T 7714 | Xia, Lian,You, Jinmao,Li, Guoliang,et al. Compositional and Antioxidant Activity Analysis of Zanthoxylum bungeanum Seed Oil Obtained by Supercritical CO2 Fluid Extraction[J]. JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY,2011,88(1):23-32. |
| APA | Xia, Lian,You, Jinmao,Li, Guoliang,Sun, Zhiwei,&Suo, Yourui.(2011).Compositional and Antioxidant Activity Analysis of Zanthoxylum bungeanum Seed Oil Obtained by Supercritical CO2 Fluid Extraction.JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY,88(1),23-32. |
| MLA | Xia, Lian,et al."Compositional and Antioxidant Activity Analysis of Zanthoxylum bungeanum Seed Oil Obtained by Supercritical CO2 Fluid Extraction".JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY 88.1(2011):23-32. |
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