NWIPB OpenIR
Simultaneous Determination of Food-Related Biogenic Amines and Precursor Amino Acids Using in Situ Derivatization Ultrasound-Assisted Dispersive Liquid-Liquid Microextraction by Ultra-High-Performance Liquid Chromatography Tandem Mass Spectrometry
He, Yongrui ; Zhao, Xian-En ; Wang, Renjun ; Wei, Na ; Sun, Jing ; Dang, Jun ; Chen, Guang ; Liu, Zhiqiang ; Zhu, Shuyun ; You, Jinmao
2016-11-02
发表期刊JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
摘要A simple, rapid, sensitive, selective, and environmentally friendly method; based on in situ derivatization ultrasound-assisted dispersive liquid-liquid microextraction (in situ DUADLLME) coupled with ultra-high-performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS) using multiple reaction monitoring (MRM) mode has been developed for the simultaneous determination of food-related biogenic amines and amino acids. A new mass-spectrometry sensitive derivatization reagent 4'-carbonyl chloride rosamine (CCR) was designed, synthesized, and first reported. Parameters and conditions of in situ DUADLLME and UHPLC-MS/MS were, optimized in detail. Under the optimized conditions, the in situ DUADLLME was completed speedily (within 1 min) with high derivatization efficiencies (>= 98.5%). With the cleanup and concentration of microextraction step, good analytical performance was obtained for the analytes. The results showed that this method was accurate and practical for quantification of biogenic amines and amino acids in common food samples (red wine, beer, wine, cheese, sausage, and fish).
文献类型期刊论文
条目标识符http://210.75.249.4/handle/363003/27769
专题中国科学院西北高原生物研究所
推荐引用方式
GB/T 7714
He, Yongrui,Zhao, Xian-En,Wang, Renjun,et al. Simultaneous Determination of Food-Related Biogenic Amines and Precursor Amino Acids Using in Situ Derivatization Ultrasound-Assisted Dispersive Liquid-Liquid Microextraction by Ultra-High-Performance Liquid Chromatography Tandem Mass Spectrometry[J]. JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY,2016.
APA He, Yongrui.,Zhao, Xian-En.,Wang, Renjun.,Wei, Na.,Sun, Jing.,...&You, Jinmao.(2016).Simultaneous Determination of Food-Related Biogenic Amines and Precursor Amino Acids Using in Situ Derivatization Ultrasound-Assisted Dispersive Liquid-Liquid Microextraction by Ultra-High-Performance Liquid Chromatography Tandem Mass Spectrometry.JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY.
MLA He, Yongrui,et al."Simultaneous Determination of Food-Related Biogenic Amines and Precursor Amino Acids Using in Situ Derivatization Ultrasound-Assisted Dispersive Liquid-Liquid Microextraction by Ultra-High-Performance Liquid Chromatography Tandem Mass Spectrometry".JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY (2016).
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