NWIPB OpenIR
独一味中Phlorigidoside C天然产物标准品制备方法及其应用
岳会兰 ; 赵晓辉 ; 于瑞涛 ; 党军 ; 邵赟 ; 梅丽娟 ; 王启兰 ; 陶燕铎
2017-04-26
Abstract本发明涉及一种独一味中Phlorigidoside#C天然产物标准品制备方法,该方法包括以下步骤:⑴样品处理:独一味全草切段后,经乙醇回流提取,即得独一味提取物;⑵溶剂萃取:独一味提取物溶解后经萃取、减压浓缩,即得正丁醇萃取物;⑶大孔树脂柱分离:正丁醇萃取物溶解后,经D101大孔树脂柱洗脱、减压浓缩得到Phlorigidoside#C粗品;⑷反相C18柱分离:Phlorigidoside#C粗品溶解后,经C18柱分离柱洗脱、减压浓缩得到初步纯化的Phlorigidoside#C;⑸反相制备HPLC纯化:初步纯化的Phlorigidoside#C溶解后,经反相制备HPLC纯化、减压浓缩,即得Phlorigidoside#C天然产物标准品。本发明工艺简单、易于操作、产品收率高且质量好,所得Phlorigidoside#C可用于治疗类风湿性关节炎。
Document Type专利
Identifierhttp://210.75.249.4/handle/363003/28403
Collection中国科学院西北高原生物研究所
Recommended Citation
GB/T 7714
岳会兰,赵晓辉,于瑞涛,等. 独一味中Phlorigidoside C天然产物标准品制备方法及其应用[P]. 2017-04-26.
Files in This Item:
There are no files associated with this item.
Related Services
Recommend this item
Bookmark
Usage statistics
Export to Endnote
Google Scholar
Similar articles in Google Scholar
[岳会兰]'s Articles
[赵晓辉]'s Articles
[于瑞涛]'s Articles
Baidu academic
Similar articles in Baidu academic
[岳会兰]'s Articles
[赵晓辉]'s Articles
[于瑞涛]'s Articles
Bing Scholar
Similar articles in Bing Scholar
[岳会兰]'s Articles
[赵晓辉]'s Articles
[于瑞涛]'s Articles
Terms of Use
No data!
Social Bookmark/Share
All comments (0)
No comment.
 

Items in the repository are protected by copyright, with all rights reserved, unless otherwise indicated.