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朱砂安神丸质量标准的探讨
曾令峰; 魏玉海; 刘学良; 王慧春; 沈建伟; 王环; 张本印; 张晓峰
2011-02-01
Source Publication中国医院药学杂志
ISSN1001-5213
Volume31Issue:2Pages:152-154
Abstract目的: 用薄层色谱法和高效液相色谱法建立朱砂安神丸定性鉴别和定量测定的方法, 建立朱砂安神丸的质量标准。方法: 黄连、当归和甘草展开系统分别采用甲苯-醋酸乙酯-甲醇-异丙醇-水(12:6:4:4:0.6),正己烷-醋酸乙酯-甲醇( 9:1:0.2)和醋酸乙酯-甲酸-冰醋酸-水(15:1:1:2) 。采用C18(4.6mm×250mm,5μm) 色谱柱, 流动相为乙腈0.05%-磷酸二氢钾(25:75),流速1.0mL?min-1,检测波长264 nm,进样量10μL, 柱温30。结果: 盐酸小檗碱进样量在0.0252-0.504μg范围内呈良好的线性关系, 回归方程Y=3971.4X+9.9657,r=0.9998(n=5).平均加样回收率为99.3%,RSD为0.69%。结论:本鉴别方法专属性强,定量方法简便可靠, 可有效控制该药的质量标准。
Indexed ByCSCD
CSCD IDCSCD:4149716
Citation statistics
Cited Times:1[CSCD]   [CSCD Record]
Document Type期刊论文
Identifierhttp://210.75.249.4/handle/363003/2996
Collection中国科学院西北高原生物研究所
Recommended Citation
GB/T 7714
曾令峰,魏玉海,刘学良,等. 朱砂安神丸质量标准的探讨[J]. 中国医院药学杂志,2011,31(2):152-154.
APA 曾令峰.,魏玉海.,刘学良.,王慧春.,沈建伟.,...&张晓峰.(2011).朱砂安神丸质量标准的探讨.中国医院药学杂志,31(2),152-154.
MLA 曾令峰,et al."朱砂安神丸质量标准的探讨".中国医院药学杂志 31.2(2011):152-154.
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