NWIPB OpenIR
Simultaneous Determination of Food-Related Biogenic Amines and Precursor Amino Acids Using in Situ Derivatization Ultrasound-Assisted Dispersive Liquid-Liquid Microextraction by Ultra-High-Performance Liquid Chromatography Tandem Mass Spectrometry
He, Yongrui1,2; Zhao, Xian-En1,2; Wang, Renjun1,2; Wei, Na1,2; Sun, Jing3,4; Dang, Jun3,4; Chen, Guang1,2; Liu, Zhiqiang5,6; Zhu, Shuyun1,2; You, Jinmao1,2,3,4
2016-11-02
发表期刊JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
卷号64期号:43页码:8225-8234
文章类型Article
摘要A simple, rapid, sensitive, selective, and environmentally friendly method; based on in situ derivatization ultrasound-assisted dispersive liquid-liquid microextraction (in situ DUADLLME) coupled with ultra-high-performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS) using multiple reaction monitoring (MRM) mode has been developed for the simultaneous determination of food-related biogenic amines and amino acids. A new mass-spectrometry sensitive derivatization reagent 4'-carbonyl chloride rosamine (CCR) was designed, synthesized, and first reported. Parameters and conditions of in situ DUADLLME and UHPLC-MS/MS were, optimized in detail. Under the optimized conditions, the in situ DUADLLME was completed speedily (within 1 min) with high derivatization efficiencies (>= 98.5%). With the cleanup and concentration of microextraction step, good analytical performance was obtained for the analytes. The results showed that this method was accurate and practical for quantification of biogenic amines and amino acids in common food samples (red wine, beer, wine, cheese, sausage, and fish).
关键词In Situ Derivatization Ultrasound-assisted Dispersive Liquid-liquid Microextraction Amino Acids Biogenic Amines Uhplc-ms/ms (Mrm)
WOS标题词Science & Technology ; Life Sciences & Biomedicine ; Physical Sciences
DOI10.1021/acs.jafc.6b03536
关键词[WOS]WINE SAMPLES ; PRECOLUMN DERIVATIZATION ; FLUORESCENCE DETECTION ; EXTRACTION ; HPLC ; BEER ; NEUROTRANSMITTERS ; BENZOYLATION ; QUANTITATION ; POLYAMINES
收录类别SCI
语种英语
项目资助者National Natural Science Foundation of China(81303179 ; Natural Science Foundation of Shandong Province(ZR2013BQ018) ; Open Funds of the State Key Laboratory of Electroanalytical Chemistry(SKLEAC201506) ; Development Project of Qinghai Key Laboratory of Qinghai-Tibet Plateau Biological Resources(2014-Z-Y3) ; Open Projects Program of the Key Laboratory of Tibetan Medicine Research, Chinese Academy of Sciences ; Foundation of Qufu Normal University(BSQD2012019 ; 31200400 ; 2012023) ; 81403051 ; 21475074 ; 21405094)
WOS研究方向Agriculture ; Chemistry ; Food Science & Technology
WOS类目Agriculture, Multidisciplinary ; Chemistry, Applied ; Food Science & Technology
WOS记录号WOS:000387095200017
引用统计
被引频次:37[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://210.75.249.4/handle/363003/6411
专题中国科学院西北高原生物研究所
作者单位1.Qufu Normal Univ, Shandong Prov Key Lab Life Organ Anal, Coll Chem & Chem Engn, Qufu 273165, Shandong, Peoples R China
2.Qufu Normal Univ, Key Lab Pharmaceut Intermediates & Anal Nat Med, Coll Chem & Chem Engn, Qufu 273165, Shandong, Peoples R China
3.Chinese Acad Sci, Qinghai Key Lab Qinghai Tibet Plateau Biol Resour, Northwest Inst Plateau Biol, Xining 810001, Qinghai, Peoples R China
4.Chinese Acad Sci, Key Lab Tibetan Med Res, Northwest Inst Plateau Biol, Xining 810001, Qinghai, Peoples R China
5.Chinese Acad Sci, Natl Ctr Mass Spectrometry Changchun, 5625 Renmin St, Changchun 130022, Peoples R China
6.Chinese Acad Sci, Key Lab Tradit Chinese Med Chem & Mass Spectromet, Changchun Inst Appl Chem, 5625 Renmin St, Changchun 130022, Peoples R China
推荐引用方式
GB/T 7714
He, Yongrui,Zhao, Xian-En,Wang, Renjun,et al. Simultaneous Determination of Food-Related Biogenic Amines and Precursor Amino Acids Using in Situ Derivatization Ultrasound-Assisted Dispersive Liquid-Liquid Microextraction by Ultra-High-Performance Liquid Chromatography Tandem Mass Spectrometry[J]. JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY,2016,64(43):8225-8234.
APA He, Yongrui.,Zhao, Xian-En.,Wang, Renjun.,Wei, Na.,Sun, Jing.,...&You, Jinmao.(2016).Simultaneous Determination of Food-Related Biogenic Amines and Precursor Amino Acids Using in Situ Derivatization Ultrasound-Assisted Dispersive Liquid-Liquid Microextraction by Ultra-High-Performance Liquid Chromatography Tandem Mass Spectrometry.JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY,64(43),8225-8234.
MLA He, Yongrui,et al."Simultaneous Determination of Food-Related Biogenic Amines and Precursor Amino Acids Using in Situ Derivatization Ultrasound-Assisted Dispersive Liquid-Liquid Microextraction by Ultra-High-Performance Liquid Chromatography Tandem Mass Spectrometry".JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY 64.43(2016):8225-8234.
条目包含的文件
条目无相关文件。
个性服务
推荐该条目
保存到收藏夹
查看访问统计
导出为Endnote文件
谷歌学术
谷歌学术中相似的文章
[He, Yongrui]的文章
[Zhao, Xian-En]的文章
[Wang, Renjun]的文章
百度学术
百度学术中相似的文章
[He, Yongrui]的文章
[Zhao, Xian-En]的文章
[Wang, Renjun]的文章
必应学术
必应学术中相似的文章
[He, Yongrui]的文章
[Zhao, Xian-En]的文章
[Wang, Renjun]的文章
相关权益政策
暂无数据
收藏/分享
所有评论 (0)
暂无评论
 

除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。