Determination of Aliphatic Amines in Infant Food Packaging Materials by High Performance Liquid Chromatography

doi:10.11895/j.issn.0253-3820.160277

NWIPB OpenIR

	Determination of Aliphatic Amines in Infant Food Packaging Materials by High Performance Liquid Chromatography
	Sheng Cun-Cun 1; Zhang Shi-Juan 1; Wang Fang-Fang 1; Ji Zhong-Yin 1; Dou Kun 1; You Jin-Mao 1,2
	2016-09-01
发表期刊	CHINESE JOURNAL OF ANALYTICAL CHEMISTRY
卷号	44 期号:9 页码:1365-1371
文章类型	Article
摘要	Aliphatic amines in infant food packaging materials were extracted and concentrated by 0. 5 mL of acidified methanol using gas purge microsyringe extraction (GP-MSE). Pre-column fluorescence labeling of amines was achieved in mild conditions with 10-ethyl-acridine-2-sulfonyl chloride (EASC) as labeling reagent. The derivatization was carried out at 60 degrees C and pH 10. The derivatives were successfully separated on a Hypersil GOLD column with excitation and emission wavelengths of 262 and 430 nm, respectively. The detection limits were in the range of 0. 4-0. 6 mu g/kg, and the quantitation limits were in the range of 1. 2-2. 1 mu g/kg. All analytes were in good linearity in the concentration range of 2. 0-2000 mu g/L with correlation coefficients of higher than 0. 998. The developed method was characterized by celerity, accuracy and high sensitivity. It was successfully applied to the determination of aliphatic amines in infant food packaging materials.
关键词	High Performance Liquid Chromatography Gas Purge-microsyringe Extraction Packaging Materials Of Baby Food Fluorescence Detection
WOS标题词	Science & Technology ; Physical Sciences
DOI	10.11895/j.issn.0253-3820.160277
关键词[WOS]	MASS-SPECTROMETRY ; AROMATIC-AMINES ; EXTRACTION ; MICROEXTRACTION ; IDENTIFICATION ; FLUORESCENCE ; CHALLENGE
收录类别	SCI
语种	英语
项目资助者	National Natural Science Foundation of China(21275089) ; Natural Science Foundation of Shandong Province, China(ZR2014BQ009)
WOS研究方向	Chemistry
WOS类目	Chemistry, Analytical
WOS记录号	WOS:000389035700007
引用统计	被引频次：4[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	http://210.75.249.4/handle/363003/6649
专题	中国科学院西北高原生物研究所
作者单位	1.Qufu Normal Univ, Coll Chem & Chem Engn, Key Lab Pharmaceut Intermediates & Anal Nat Med, Shandong Prov Key Lab Life Organ Anal, Qufu 273165, Peoples R China 2.Chinese Acad Sci, Northwest Inst Plateau Biol, Xining 810001, Peoples R China
推荐引用方式 GB/T 7714	Sheng Cun-Cun,Zhang Shi-Juan,Wang Fang-Fang,et al. Determination of Aliphatic Amines in Infant Food Packaging Materials by High Performance Liquid Chromatography[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2016,44(9):1365-1371.
APA	Sheng Cun-Cun,Zhang Shi-Juan,Wang Fang-Fang,Ji Zhong-Yin,Dou Kun,&You Jin-Mao.(2016).Determination of Aliphatic Amines in Infant Food Packaging Materials by High Performance Liquid Chromatography.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,44(9),1365-1371.
MLA	Sheng Cun-Cun,et al."Determination of Aliphatic Amines in Infant Food Packaging Materials by High Performance Liquid Chromatography".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 44.9(2016):1365-1371.