Knowledge Management System of Northwest Institute of Plateau Biology, CAS
Separation of three anthraquinone glycosides including two isomers by preparative high-performance liquid chromatography and high-speed countercurrent chromatography from Rheum tanguticum Maxim. ex Balf | |
Chen, Tao1,2; Li, Hongmei1,2,3; Zou, Denglang1,2,3; Liu, Yongling1,2; Chen, Chen1,2; Zhou, Guoying1,2; Li, Yulin1,2 | |
2016-08-01 | |
发表期刊 | JOURNAL OF SEPARATION SCIENCE |
卷号 | 39期号:16页码:3105-3112 |
文章类型 | Article |
摘要 | Anthraquinone glycosides, such as chrysophanol 1-O--d-glucoside, chrysophanol 8-O--d-glucoside, and physion 8-O--d-glucoside, are the accepted important active components of Rheum tanguticum Maxim. ex Balf. due to their pharmacological properties: antifungal, antimicrobial, cytotoxic, and antioxidant activities. However, an effective method for the separation of the above-mentioned anthraquinone glycosides from this herb is not currently available. Especially, greater difficulty existed in the separation of the two isomers chrysophanol 1-O--d-glucoside and chrysophanol 8-O--d-glucoside. This study demonstrated an efficient strategy based on preparative high-performance liquid chromatography and high-speed countercurrent chromatography for the separation of the above-mentioned anthraquinone glycosides from Rheum tanguticum Maxim.ex Balf. |
关键词 | Anthraquinone Glycosides High-speed Countercurrent Chromatography Isomers Preparative High-performance Liquid Chromatography Rheum Tanguticum Maxim Ex Balf |
WOS标题词 | Science & Technology ; Physical Sciences |
DOI | 10.1002/jssc.201600487 |
关键词[WOS] | MASS-SPECTROMETRY ; MACROPOROUS RESIN ; RAPID ENRICHMENT ; SCALE-UP ; PURIFICATION ; HPLC ; RHUBARB ; CONSTITUENTS ; EXTRACTION ; EMODI |
收录类别 | SCI |
语种 | 英语 |
项目资助者 | Strategic Pilot Science and Technology Project of CAS(XDA12050304) ; General Program of Natural Science Foundation of Qinghai Province(2015-ZJ-908) ; Science and Technology Support Program of Qinghai Province(2015-NS-115) ; Instrument Function Development Project of CAS(2017g107) |
WOS研究方向 | Chemistry |
WOS类目 | Chemistry, Analytical |
WOS记录号 | WOS:000383361800002 |
引用统计 | |
文献类型 | 期刊论文 |
条目标识符 | http://210.75.249.4/handle/363003/6450 |
专题 | 中国科学院西北高原生物研究所 |
作者单位 | 1.Chinese Acad Sci, Northwest Inst Plateau Biol, Key Lab Tibetan Med Res, Xining, Peoples R China 2.Chinese Acad Sci, Northwest Inst Plateau Biol, Key Lab Adaptat & Evolut Plateau Biota, Xining, Peoples R China 3.Univ Chinese Acad Sci, Beijing, Peoples R China |
推荐引用方式 GB/T 7714 | Chen, Tao,Li, Hongmei,Zou, Denglang,et al. Separation of three anthraquinone glycosides including two isomers by preparative high-performance liquid chromatography and high-speed countercurrent chromatography from Rheum tanguticum Maxim. ex Balf[J]. JOURNAL OF SEPARATION SCIENCE,2016,39(16):3105-3112. |
APA | Chen, Tao.,Li, Hongmei.,Zou, Denglang.,Liu, Yongling.,Chen, Chen.,...&Li, Yulin.(2016).Separation of three anthraquinone glycosides including two isomers by preparative high-performance liquid chromatography and high-speed countercurrent chromatography from Rheum tanguticum Maxim. ex Balf.JOURNAL OF SEPARATION SCIENCE,39(16),3105-3112. |
MLA | Chen, Tao,et al."Separation of three anthraquinone glycosides including two isomers by preparative high-performance liquid chromatography and high-speed countercurrent chromatography from Rheum tanguticum Maxim. ex Balf".JOURNAL OF SEPARATION SCIENCE 39.16(2016):3105-3112. |
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