Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry

NWIPB OpenIR

	Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry
	Cai, Yiping ; Sun, Zhiwei ; Chen, Guang ; Liu, Xiaomei ; You, Jinmao ; Zhang, Caiqing
	2016-02-01
发表期刊	FOOD CHEMISTRY
摘要	A pair of isotope-coded derivatization reagents, d(0)-10-methyl-acridone-2-sulfonyl chloride (d(0)-MASC, light form) and d(3)-10-methyl-acridone-2-sulfonyl chloride (d(3)-MASC, heavy form), were used for labeling biogenic amines (BAs). On basis of the isotope-coded derivatization, a global isotope internal standard quantitative method for determining seven BAs by high-performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) was developed. The d(0)-MASC and d(3)-MASC can easily label BAs under mild conditions within 15 min at 50 degrees C. The obtained light and heavy labeled BAs were monitored by the transitions of [M+H](+) -> 208 and [M+H](+) -> 211, respectively. Relative quantification of BAs was achieved by calculation of the peak area ratios of d(0)-MASC/d(3)-MASC labeled derivatives. Excellent linear responses for relative quantification were observed in the range of 1/10-10/1. The developed method has been successfully applied to the quantification of BAs in Chinese rice wine with recoveries ranging from 94.9% to 104.5%. (C) 2015 Elsevier Ltd. All rights reserved.
文献类型	期刊论文
条目标识符	http://210.75.249.4/handle/363003/53334
专题	中国科学院西北高原生物研究所
推荐引用方式 GB/T 7714	Cai, Yiping,Sun, Zhiwei,Chen, Guang,et al. Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry[J]. FOOD CHEMISTRY,2016.
APA	Cai, Yiping,Sun, Zhiwei,Chen, Guang,Liu, Xiaomei,You, Jinmao,&Zhang, Caiqing.(2016).Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry.FOOD CHEMISTRY.
MLA	Cai, Yiping,et al."Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry".FOOD CHEMISTRY (2016).