Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry

NWIPB OpenIR

	Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry
	Cai, Yiping 1; Sun, Zhiwei 1; Chen, Guang 2; Liu, Xiaomei 2; You, Jinmao 2,3; Zhang, Caiqing 4
	2016-02-01
发表期刊	FOOD CHEMISTRY
卷号	192 页码:388-394
文章类型	Article
摘要	A pair of isotope-coded derivatization reagents, d(0)-10-methyl-acridone-2-sulfonyl chloride (d(0)-MASC, light form) and d(3)-10-methyl-acridone-2-sulfonyl chloride (d(3)-MASC, heavy form), were used for labeling biogenic amines (BAs). On basis of the isotope-coded derivatization, a global isotope internal standard quantitative method for determining seven BAs by high-performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) was developed. The d(0)-MASC and d(3)-MASC can easily label BAs under mild conditions within 15 min at 50 degrees C. The obtained light and heavy labeled BAs were monitored by the transitions of [M+H](+) -> 208 and [M+H](+) -> 211, respectively. Relative quantification of BAs was achieved by calculation of the peak area ratios of d(0)-MASC/d(3)-MASC labeled derivatives. Excellent linear responses for relative quantification were observed in the range of 1/10-10/1. The developed method has been successfully applied to the quantification of BAs in Chinese rice wine with recoveries ranging from 94.9% to 104.5%. (C) 2015 Elsevier Ltd. All rights reserved.
关键词	Biogenic Amines (Bas) High-performance Liquid Chromatography-tandem Mass Spectrometry (Hplc-ms/ms) Isotope-coded Derivatization Reagent Chinese Rice Wine
WOS标题词	Science & Technology ; Physical Sciences ; Life Sciences & Biomedicine
关键词[WOS]	FLUORESCENCE DETECTION ; FOODS ; SAMPLES ; CHEESE
收录类别	SCI
语种	英语
WOS研究方向	Chemistry ; Food Science & Technology ; Nutrition & Dietetics
WOS类目	Chemistry, Applied ; Food Science & Technology ; Nutrition & Dietetics
WOS记录号	WOS:000362304500052
引用统计	被引频次：34[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	http://210.75.249.4/handle/363003/6528
专题	中国科学院西北高原生物研究所
作者单位	1.Qufu Normal Univ, Key Lab Life Organ Anal Shandong Prov, Qufu 273165, Peoples R China 2.Key Lab Pharmaceut Intermediates & Nat Prod, Qufu 273165, Peoples R China 3.Chinese Acad Sci, Northwest Inst Plateau Biol, Xining, Peoples R China 4.Shandong Univ, Qianfoshan Hosp, Jinan 250100, Peoples R China
推荐引用方式 GB/T 7714	Cai, Yiping,Sun, Zhiwei,Chen, Guang,et al. Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry[J]. FOOD CHEMISTRY,2016,192:388-394.
APA	Cai, Yiping,Sun, Zhiwei,Chen, Guang,Liu, Xiaomei,You, Jinmao,&Zhang, Caiqing.(2016).Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry.FOOD CHEMISTRY,192,388-394.
MLA	Cai, Yiping,et al."Rapid analysis of biogenic amines from rice wine with isotope-coded derivatization followed by high performance liquid chromatography-tandem mass spectrometry".FOOD CHEMISTRY 192(2016):388-394.